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              Leak Testing 
               
              Getting 
              down to the fundamentals of leak detection & measurement 
            Featured in Medical Device Technology 
            May 2002 Leak testing 
            can be separated into two fundamental disciplines.  
            Leak detection, 
              in which the value of the leakage rate is generally nonquantifiable, 
              and leak measurement, in which techniques 
              are used to record the rate of leakage.  
              
            Leak detection 
            The common feature of methods used to detect leaks is that they 
              are almost always operator-dependent, require strict supervision 
              and are often very messy. The methods listed below will indicate 
              a leak condition, but they will not accurately quantify the degree 
              of leakage. 
            Observation. 
              Components are filled with pressurised gas and immersed in 
              a liquid. Typically they are filled with air and immersed in water, 
              but nitrogen under acetone is also used. The most common observation 
              technique is to look for a bubble stream. A variation of the bubble-stream 
              method is to use sealed components submerged in a liquid within 
              an enclosed volume; a vacuum is created at the surface of the liquid 
              to draw the fluid into the closed device. This method is often used 
              to soak-test parts over a prolonged period and then to visually 
              check for condensation inside transparent parts. It is also used 
              to check the weight of parts to ensure that product, that is, the 
              powder, gas or liquid inside the device, has not been forced out 
              and vapour/liquid has not been forced inside.  
            Chemical trace. Chemicals 
              are added to the working media within an assembly prior to some 
              form of functional test. If they leak onto the surface of the component, 
              they can be readily seen when viewed using ultraviolet light. 
            Chemical penetration. 
              Chemical is sprayed onto one side of a component and by capillary 
              action emerges on the opposite surface. This technique is also referred 
              to as dye penetration. The difference between chemical trace and 
              dye penetration is that the former is a trace substance in the fluid 
              whereas the latter is coated onto the surface of the container. 
            Gas sniffing. Components 
              or assemblies are filled or injected with an easily identifiable 
              gas to create a pressure differential. Helium, hydrogen and sulphur 
              hexafluoride (SF6) gases are employed and an operator searches for 
              concentrations of gas at the surface of the piece being tested. 
              Helium is the most commonly used.SF6 is generally avoided whenever 
              possible because of its toxicity, but it is mandatory for some electrical 
              equipment because of its flame-suppression properties. For sealed 
              assemblies such as blister packs or swallowable cameras, the item 
              must be closed in an environment containing the tracer gas. 
            Ultrasonic testing. 
              Because they are noisy, large gas flows can be found using an ultrasonic 
              detector. This method is suited to finding large leaks, but it is 
              not recommended for the fine leaks in a production environment. 
              When using ultrasonic testing, sources of misleading indications 
              and other problems can include low test pressures and capillary 
              action sealing, high-pressure situations and component damage, contaminated 
              liquids, and preferential leeching and rogue surface tensions. 
              
            Leak measurement  
            Leak measurement attempts to quantify the flow of the fluid over 
              a period of time. There are three commonly used fundamental techniques 
              for leak measurement: a pressure change within a known volume, a 
              direct measurement of flow, or measurements of changes in concentration. 
            Pressure measurement  
            Absolute measurement. A 
              transducer or gauge is used to measure pressure change within the 
              device being tested. In general, this technique is difficult to 
              apply because small changes in pressure are being measured. The 
              sensitivity of the transducer as a percentage of the full scale 
              becomes an issue because the pressure differences can be extremely 
              small even when trying to detect a large leak. 
            Reference comparison or differential 
              pressure technique. This technique involves 
              locating the test and reference volumes either side of a transducer 
              diaphragm. Ideally, these volumes should have similar pneumatic 
              characteristics, and they are arranged to be as stable as possible 
              and at the same pressure. Subsequent time-related changes in the 
              pressure of the test volume are used to measure the value of any 
              leakage. A differential pressure transducer is placed across the 
              two volumes. The sensitivity of the transducer is not related to 
              the actual pressure in absolute or gauge pressure terms, but to 
              the sensitivity of the differential pressure transducer at the test 
              pressure. For example, it is possible to detect 0.0005% of the test 
              pressure using this technique by testing at 1 bar gauge (2 bar absolute).This 
              may be 100 times more sensitive than using the absolute measurement 
              technique mentioned above. 
            Differential pressure component 
              dosing. This technique involves investigating 
              sealed components. In this technique, twin tandem pressurization 
              and reference volumes are used together with the sequential application 
              of a differential pressure transducer. It is designed to identify 
              gross leaks in sealed parts. The differential pressure technique 
              alone will not differentiate between a good part and a gross leaking 
              part; dosing is used with the differential pressure technique to 
              detect the gross leaking parts.  
            Inter-stream testing. 
              Two test pressures and three interrelated differential 
              pressure transducers are used to simultaneously test two adjacent 
              volumes. This technique is used when there are two fluid volumes 
              in a single part, which could leak to the outside or between each 
              other. 
            Continuous flow  
            Controlled pressure. 
              This involves creating a prescribed pressure within the product 
              being tested and then measuring the gas flow that is needed to maintain 
              that pressure using a flow measurement transducer. 
            Free flow.This 
              technique introduces a flow-measurement device into the gas stream. 
            Gas trace  
            Gas tracer systems have the ability to detect smaller leakages, 
              but tend to require higher capital investment. 
            Helium. This 
              requires enclosing the test piece within a sealed chamber and evacuating 
              the chamber and/or test piece. After charging one or the other with 
              helium, the gas loss from the respective volume is monitored with 
              a mass spectrometer that detects the helium. 
            Hydrogen. This 
              gas is used in the same way as helium. It is also used in a technique 
              that employs a sensor to detect and measure levels of, in this case, 
              hydrogen in a continuous ambient or low pressure gas flow, which 
              allows the use of lower cost enclosures and ducting. The test gas 
              is a mixture of 95% nitrogen and 5% hydrogen, which is nonexplosive 
              and relatively inexpensive. 
            Gas bombing. This 
              involves exposing a sealed component to a gas-charged environment 
              and subsequent transfer to a test chamber that is monitored by gas 
              sensing instrumentation. It is essential that the possibility of 
              a gross leak is eliminated before fine leak measurement is attempted. 
            Various halogens can be used in all of the above techniques, but 
              they are avoided if possible. In addition to toxicity, they are 
              heavy gases that tend to accumulate readily in low recesses. As 
              a result, contamination occurs and the test area is difficult to 
              clear; this is made worse by the tendency of these gases to adhere 
              to surfaces.All gases will stick to the tooling surface to some 
              degree, most particularly when flooded from a leaking component. 
              However, hydrogen and helium are lighter and they are more easily 
              removed or dispersed by extraction, flushing or natural diffusion. 
             
              
            Summary. 
               
            There are a variety of leak testing techniques 
              in use today.When considering an item requiring leak testing it 
              is important to ascertain first whether detection of the leak or 
              measurement of the leakage rate is more important. Quantifying the 
              leakage rate will dictate the leak measurement technique that is 
              required.  
              
              
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